Inorganic Substances as Additives in the Marine Aquarium



John W. Linville, D.V.M.



As an alternative to commercial trace element additives, I would like to detail the possibility of making one's own solutions of the most common trace elements: calcium, strontium, iodine and bicarbonate.







Part I: Chemistry, do I really need it?

In order to better understand some of the concepts of inorganic chemistry in the marine aquarium, I want to outline some basic chemical principals applied in this article. It is not necessarily vital to understand or read this section, but it will help in following some of the ideas and math. This section is hardly meant to make chemists out of anyone. If anything, it is more of a repetition to bring back that long lost loving feeling for atoms, molecules, and the like.



Molecules:

Chemical compounds consist of molecules made up out of atoms. When these compounds are dissolved in water they separate into ions that are either positively or negatively charged. The charge is dependent upon whether an atom gives up or receives one or more electrons. This is done to reach a more stabile state. For example sodium chloride (NaCl) dissociates into a positive sodium ion (Na+) and a negative chloride ion (Cl-) in water.



Weights:

Each chemical element (or atom) has a characteristic weight. The molecular weight of a compound is thus calculated by adding the individual weights of the atoms in the molecule. This weight -- in grams -- is based on one mole of the substance, which contains a constant number of molecules. For example sodium (Na) weighs 22.9898 grams per mole, and chlorine (Cl) weighs 35.453 grams per mole. Thus the combination of the two, sodium chloride (NaCl), weighs 58.4428 grams per mole. These weights can be found in a table of chemical elements called the Periodic Table of the Elements.



Chemical Reactions:

Molecules react with each other in predictable ways. Energy and mass cannot be lost and so it is possible to know how two or more substances will react with each other. By setting up an equation and balancing out both sides, it is known what substances are available for a reaction. Making sure that both sides are equal in number of the same atoms though is important. For example, if one mole of calcium chloride (CaCl2) is dissolved in water, it dissociates into one mole of Ca2+ and two moles of Cl-. Furthermore if one mole of sodium bicarbonate (NaHCO3; baking soda) is added to the solution, it will dissociate into one mole Na+ and one mole of HCO3-.

By forming the equations for the reactions one can determine what the results will be, when added to water:

CaCl2 <==> Ca2+ + 2Cl-

NaHCO3 <==> Na+ + HCO3-

Calcium chloride has two chloride ions. Calcium has a double positively charge that can only be balanced out by two chloride ions with their single negative charges. Sodium and bicarbonate ions each have opposite single charges. This means that sodium bicarbonate consists of only one each of the ions.

If both reactions run in the same medium, the following would result:

CaCl2 + 2NaHCO3 <==> Ca(HCO3)2 + 2NaCl

Two sodium bicarbonates are needed on the left because the double positively charged calcium ion reacts with two single negatively charged bicarbonates. Conversely since two single negatively charged chloride ions are available from the calcium chloride on the left, two single charged sodium ions are needed to balance them out. A close look at the equation will show that there is the same number of ions on both sides of the double arrow.

Note: The double arrow signifies that the reaction can run in both directions.



Concentrations:

The concentration of dissolved chemicals is usually given in one of two forms. The first being "percentage." This form can either be a "weight to volume" or "volume to volume" percentage. The second form is the "molar" form. In this form the number of moles of the substance is given per 1000ml (1 liter) of solution. An example for the first form would be a 10% NaCl solution. Here 10g of NaCl are dissolved in 100ml of water (weight / volume %). Another would be a 3% vinegar solution, where 3ml of vinegar are dissolved in 100ml of water (volume / volume %). An example of a molar solution would be a one (1) molar NaCl solution. Here one (1) mole of NaCl (approximately 58.4g) is dissolved in 1000ml (1 liter) of water. A two (2) molar solution would have two (2) moles per liter, etc. Knowing the concentration enables one to calculate exactly how much substance one is adding to the aquarium in a given amount of solution.



With or Without Water? :

When buying chemical compounds, especially the ones we will be working with, knowing that some are hygroscopic is important, meaning that they attract -- or bind -- water. This is normally apparent by the fact they will clump up in damp environments. This on the one hand makes it difficult to measure them accurately and on the other hand changes the weight of the molecules, making calculations based on the original molecule invalid. One example would be calcium chloride (CaCl2), a compound we will be using. When buying this substance, it is imperative to know whether you are buying anhydrous, dihydrous or hexahydrous compounds. Anhydrous CaCl2 has a weight of 110.986 g/mole, since Ca weighs 40.08 g/mole and Cl weighs 35.453 g/mole. The dihydrate form has two (2) waters added to this weight. This means that one mole of this form weighs 147.0168 grams per mole, or 36.0308 grams per mole more (water weighs 18.0154 grams per mole). The result being that if one makes their calculations based on the anhydrous form and adds dihydrate, less calcium would be added to the system than intended. This would be even more drastic with the hexahydrate form, as it has six (6) waters added.

Note: Bound water is signified by a "dot" between the chemical formula for the substance and the number of waters bound. For example, the dihydrous form of calcium chloride: CaCl2.2H2O



Chemical Purity:

There are also different grades of purity on the market. While each person must decide for himself how much impurity they can tolerate, beware of phosphates and copper especially. Buying cheaper grades of chemical may seem great at first, but can be the root cause of inexplicable algae blooms or invertebrate die-offs.



Again, this was not meant to make chemists out of anyone. If it has piqued your interest in the subject, please refer to any number of good general chemistry books, such as the one from Charles E. Mortimer.



This was the first part of three part series on making one's own trace element additives. The next installment will have the actual "cook book recipes" for the solutions and their approximate dosages.

Part II: Inorganic Substances as Additives in the Marine Aquarium

Part III: Inorganic Substances as Additives in the Marine Aquarium